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It was also found that the C2 selectivity decreases almost linearly with increasing methane conversion, usually achieved by increasing the oxygen concentration in the feed This is formulated as the "100% rule,,,295 indicating that methane conversion and C 2 selectivity roughly sum to 100% At low conversions, using reaction mixtures of high C~ : O2 ratio, selectivities of ::;70% may be obtained In fixed-bed flow reactors a C2 selectivity of 50% may be achieved at a conversion level of 40% at atmospheric pressure 12 C2 yields in the range 20-25% are usually achieved A C2 yield slightly better than 50% (80% selectivity at 65% methane conversion, above 700 C, Sm203 catalyst), however, has been reported 28 A special technique, a separative chemical reactor simulating a countercurrent chromatographic moving bed has been applied.
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Another technical modification has resulted in even higher yields 29 In this case methane coupling is carried out in a gas recycle electrocatalytic or catalytic reactor over silver catalysts (800 C, Ag on Y20rZr02 or Ag on Sm203 doped with CaO) and the recycle gas passes through a Linde 5A molecular sieve at 30 C The adsorbed C2 hydrocarbons, which are trapped and therefore protected from further oxidation, are subsequently desorbed at 400 C The method ensures high yields and selectivities (total yields up to 88%, ethylene yields ::;85%, ethylene selectivities ::;88% for methane conversion ::;97%) At present, there is a general agreement that the primary function of the catalysts in oxidative coupling of methane is to form methyl radicals.
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result. However, the error string might be overwritten or deallocated by subsequent calls to other SQLite interface functions. When serialized threading mode is in use, a second error may occur on a separate thread between the time of the rst error and the call to these interfaces. When that happens, the second error is reported since these interfaces always report the most recent result. To avoid this, each thread can obtain exclusive use of database connection D by invoking sqlite3_mutex_enter(sqlite3_db_ mutex(D)) before beginning to use D and invoking sqlite3_mutex_ leave(sqlite3_db_mutex(D)) after all calls to the interfaces listed here are complete. If an interface fails with SQLITE_MISUSE, the interface was invoked incorrectly by the application. In that case, the error code and message may or may not be set. A full list of result codes and extended result codes (used for I/O errors) can be found on the SQLite website at www.sqlite. org/c3ref/c abort.html .
Considerable evidence attained by electron paramagnetic resonance,313,330 mass spectroscopy,331 and isotopic labeling studies332-334 indicates that methyl radicals produced in a heterogeneous process are the primary intermediate in the production of ethane Methyl radicals are formed in a direct route with the involvement of surface oxygen (Os -) [Eq (328)] Alternatively, an acid-base process with the interaction of oxygen ions of low coordination number (0;-) with methane may form a methyl anion that then reacts further with molecular oxygen to give methyl radica1335-337 [Eq (329)]:.
Figure 28-2: The Library Item Property inspector identifies the source file for any selected Library entry. You can also see evidence of Library items in the HTML for the current page. Open the Code inspector, and you see that several lines of code have been added. The following code example indicates one Library item:
Suppose that you declare a method that takes two parameters. Whenever you call this method, you need to pass two parameters along with it.
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